Optimization of extraction parameters for the chemical profiling of 3,4-methylenedioxymethamphetamine (MDMA) tablets
| dc.contributor.author | Pascal Gimeno | |
| dc.contributor.author | Fabrice Besacier | |
| dc.date.accessioned | 2012-11-07T09:19:37Z | |
| dc.date.accessioned | 2025-02-17T13:59:25Z | |
| dc.date.available | 2012-11-07T09:19:37Z | |
| dc.date.issued | 2012-11-07 | |
| dc.description | The extraction of impurities from illegally produced 3,4-methylenedioxymethamphetamine (MDMA) has been studied in order to optimize the parameters. Two different MDMA samples were used. Particular attention was paid to the influence of the pH, the evaporation step, and the sample storage. The method used was an extraction of impurities by diethyl ether from a buffer solution at pH 11.5, followed by gas chromatography (GC) mass spectrometric (MS) analyses after a dryness concentration under monitored conditions of the ethereal extract. Repeat extractions of the same sample gave an average relative standard deviation (RSD) of less than 8.5% within day and less than 10.5% between days. # 2003 Elsevier Science Ireland Ltd. All rights reserved. | en_US |
| dc.description.abstract | The extraction of impurities from illegally produced 3,4-methylenedioxymethamphetamine (MDMA) has been studied in order to optimize the parameters. Two different MDMA samples were used. Particular attention was paid to the influence of the pH, the evaporation step, and the sample storage. The method used was an extraction of impurities by diethyl ether from a buffer solution at pH 11.5, followed by gas chromatography (GC) mass spectrometric (MS) analyses after a dryness concentration under monitored conditions of the ethereal extract. Repeat extractions of the same sample gave an average relative standard deviation (RSD) of less than 8.5% within day and less than 10.5% between days. # 2003 Elsevier Science Ireland Ltd. All rights reserved. | en_US |
| dc.identifier.uri | https://dl.ftveti.edu.et/handle/123456789/3919 | |
| dc.language.iso | en | en_US |
| dc.subject | 3,4-Methylenedioxymethamphetamine (MDMA); Impurities; Gas chromatography; Mass spectrometry; Profiling | en_US |
| dc.title | Optimization of extraction parameters for the chemical profiling of 3,4-methylenedioxymethamphetamine (MDMA) tablets | en_US |
| dc.type | Article | en_US |
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